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Both ranitidine hydrochloride form 1 and form 2 were milled separately in an oscillatory ball mill Mixer Mill MM301 Retsch Co Germany at 30 Hz A 1 g powder sample was placed in a 25 mL volume stainless steel milling jar containing two 12 mm diameter stainless steel balls.
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A mill is a device that breaks solid materials into smaller pieces by grinding crushing or cutting Such comminution is an important unit operation in many processes.There are many different types of mills and many types of materials processed in them Historically mills were powered by hand or by animals e.g via a hand crank working animal e.g horse mill wind or water .
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Grinding balls for MM 301 20 mm Ø 25 mm Ø 30 mm Ø Material Zirconium oxide 05.368.0093 05.368.0106 05.368.0092 Stainless steel 05.368.0062 05.368.0105 05.368.0061 Retsch Co KG Rheinische Straße 36 D 42781 Haan Germany Telephone 49 21 29/55 61 0 Telefax 49 21 29/87 02 E mail info retsch Internet retsch
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Effect of milling conditions on the solid state conversion
Both ranitidine hydrochloride form 1 and form 2 were milled separately in an oscillatory ball mill Mixer Mill MM301 Retsch Co Germany at 30 Hz A 1 g powder sample was placed in a 25 mL volume stainless steel milling jar containing two 12 mm diameter stainless steel balls.
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An oscillatory ball mill Mixer Mill MM301 Rets ch Gm bH Co Germany was used for cryo milling as follows 1 g of indomethacin was placed into a 25 m L milling jar and m illed with two
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An oscillatory ball mill Mixer Mill MM301 Retsch Co Germany was used for cryo milling as follows 1 g of indomethacin was placed into a 25 mL milling jar and milled with two 12 mm balls for 120 minutes The jars were immersed in liquid nitrogen for 3 min before milling and repeatedly for 3
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Briefly the samples were prepared by adding a total mass of 500 mg of the appropriate amount of DTX BIC or DTX and BIC at a 1 1 molar ratio in 25 mL milling jars using two stainless steel balls with a diameter of 12 mm and subsequent milling for a duration of 120 min at 30 Hz in a cold room at 6 °C using an oscillatory ball mill
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